Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity

Nicolay Yu Adonin; Sergey A. Prikhod’ko; Anton Yu Shabalin; Igor P. Prosvirin; Vladimir I. Zaikovskii; Dmitry I. Kochubey; Dmitry A. Zyuzin; Valentin N. Parmon; Evgeny A. Monin; Irina A. Bykova; Petr O. Martynov; Sergey L. Rusakov; Pavel A. Storozhenko

doi:10.1007/s12633-014-9272-5

Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity

Nicolay Yu Adonin, Sergey A. Prikhod’ko, Anton Yu Shabalin, Igor P. Prosvirin, Vladimir I. Zaikovskii, Dmitry I. Kochubey, Dmitry A. Zyuzin, Valentin N. Parmon, Evgeny A. Monin, Irina A. Bykova, Petr O. Martynov, Sergey L. Rusakov, Pavel A. Storozhenko

Лаборатория синтеза и исследования новых материалов для ресурсосберегающих каталитических и адсорбционных процессов ФЕН
Кафедра физических методов исследования твердого тела ФФ

Результат исследования: Научные публикации в периодических изданиях › статья

1 Цитирования (Scopus)

Аннотация

A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl₂⋅2H₂O and Cu(OH)₂ mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.

Язык оригинала	английский
Страницы (с-по)	79-87
Число страниц	9
Журнал	Silicon
Том	7
Номер выпуска	2
DOI	https://doi.org/10.1007/s12633-014-9272-5
Состояние	Опубликовано - 18 апр 2015

Доступ к документу

10.1007/s12633-014-9272-5

Link to publication in Scopus

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Цитировать

Adonin, N. Y., Prikhod’ko, S. A., Shabalin, A. Y., Prosvirin, I. P., Zaikovskii, V. I., Kochubey, D. I., Zyuzin, D. A., Parmon, V. N., Monin, E. A., Bykova, I. A., Martynov, P. O., Rusakov, S. L., & Storozhenko, P. A. (2015). Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity. Silicon, 7(2), 79-87. https://doi.org/10.1007/s12633-014-9272-5

Adonin, Nicolay Yu ; Prikhod’ko, Sergey A. ; Shabalin, Anton Yu ; Prosvirin, Igor P. ; Zaikovskii, Vladimir I. ; Kochubey, Dmitry I. ; Zyuzin, Dmitry A. ; Parmon, Valentin N. ; Monin, Evgeny A. ; Bykova, Irina A. ; Martynov, Petr O. ; Rusakov, Sergey L. ; Storozhenko, Pavel A. / Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity. В: Silicon. 2015 ; Том 7, № 2. стр. 79-87.

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title = "Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity",

abstract = "A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl2⋅2H2O and Cu(OH)2 mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.",

keywords = "Copper catalyst, Cuprous chloride, Direct synthesis, Nanoparticles, Nanostructured, Silicon, Trialkoxysilanes, Triethoxysilane",

author = "Adonin, {Nicolay Yu} and Prikhod{\textquoteright}ko, {Sergey A.} and Shabalin, {Anton Yu} and Prosvirin, {Igor P.} and Zaikovskii, {Vladimir I.} and Kochubey, {Dmitry I.} and Zyuzin, {Dmitry A.} and Parmon, {Valentin N.} and Monin, {Evgeny A.} and Bykova, {Irina A.} and Martynov, {Petr O.} and Rusakov, {Sergey L.} and Storozhenko, {Pavel A.}",

year = "2015",

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doi = "10.1007/s12633-014-9272-5",

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Adonin, NY , Prikhod’ko, SA , Shabalin, AY , Prosvirin, IP , Zaikovskii, VI, Kochubey, DI, Zyuzin, DA, Parmon, VN, Monin, EA, Bykova, IA, Martynov, PO, Rusakov, SL & Storozhenko, PA 2015, 'Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity', Silicon, том. 7, № 2, стр. 79-87. https://doi.org/10.1007/s12633-014-9272-5

Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity. / Adonin, Nicolay Yu ; Prikhod’ko, Sergey A.; Shabalin, Anton Yu ; Prosvirin, Igor P.; Zaikovskii, Vladimir I.; Kochubey, Dmitry I.; Zyuzin, Dmitry A.; Parmon, Valentin N.; Monin, Evgeny A.; Bykova, Irina A.; Martynov, Petr O.; Rusakov, Sergey L.; Storozhenko, Pavel A.

В: Silicon, Том 7, № 2, 18.04.2015, стр. 79-87.

Результат исследования: Научные публикации в периодических изданиях › статья

TY - JOUR

T1 - Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity

AU - Adonin, Nicolay Yu

AU - Prikhod’ko, Sergey A.

AU - Shabalin, Anton Yu

AU - Prosvirin, Igor P.

AU - Zaikovskii, Vladimir I.

AU - Kochubey, Dmitry I.

AU - Zyuzin, Dmitry A.

AU - Parmon, Valentin N.

AU - Monin, Evgeny A.

AU - Bykova, Irina A.

AU - Martynov, Petr O.

AU - Rusakov, Sergey L.

AU - Storozhenko, Pavel A.

PY - 2015/4/18

Y1 - 2015/4/18

N2 - A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl2⋅2H2O and Cu(OH)2 mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.

AB - A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl2⋅2H2O and Cu(OH)2 mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.

KW - Copper catalyst

KW - Cuprous chloride

KW - Direct synthesis

KW - Nanoparticles

KW - Nanostructured

KW - Silicon

KW - Trialkoxysilanes

KW - Triethoxysilane

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M3 - Article

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VL - 7

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EP - 87

JO - Silicon

JF - Silicon

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