Specific features of the phase formation, synthesis, and growth of ZnMoO4 crystals

E. N. Galashov; P. S. Galkin; P. E. Plusnin; V. N. Shlegel

doi:10.1134/S1063774514020084

Specific features of the phase formation, synthesis, and growth of ZnMoO₄ crystals

E. N. Galashov, P. S. Galkin, P. E. Plusnin, V. N. Shlegel

Отдел прикладной физики ФФ

Результат исследования: Научные публикации в периодических изданиях › статья › рецензирование

10 Цитирования (Scopus)

Аннотация

The ZnO-MoO₃ phase diagram in the range of ZnO compositions from 0.95 to 1.05 mol % is refined by differential scanning calorimetry. Data on crystal stoichiometry are obtained using the weighting method by reducing ZnMoO₄ in a hydrogen atmosphere. The specific features of solid-phase synthesis of ZnMoO₄ are studied, and its heat of fusion is measured. The modes of solid-phase synthesis and growth of ZnMoO₄ crystals are optimized. Some experimental data on the ZnMoO₄ crystal growth in the [001] direction by the low-thermal gradient Czochralski method are presented. Crystals with a cross section of ∼50 × 50 mm², a length of 160 mm, and a weight up to 1 kg have been obtained.

Язык оригинала	английский
Страницы (с-по)	288-290
Число страниц	3
Журнал	Crystallography Reports
Том	59
Номер выпуска	2
DOI	https://doi.org/10.1134/S1063774514020084
Состояние	Опубликовано - мар. 2014

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abstract = "The ZnO-MoO3 phase diagram in the range of ZnO compositions from 0.95 to 1.05 mol % is refined by differential scanning calorimetry. Data on crystal stoichiometry are obtained using the weighting method by reducing ZnMoO4 in a hydrogen atmosphere. The specific features of solid-phase synthesis of ZnMoO4 are studied, and its heat of fusion is measured. The modes of solid-phase synthesis and growth of ZnMoO4 crystals are optimized. Some experimental data on the ZnMoO4 crystal growth in the [001] direction by the low-thermal gradient Czochralski method are presented. Crystals with a cross section of ∼50 × 50 mm2, a length of 160 mm, and a weight up to 1 kg have been obtained.",

author = "Galashov, {E. N.} and Galkin, {P. S.} and Plusnin, {P. E.} and Shlegel, {V. N.}",

year = "2014",

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Specific features of the phase formation, synthesis, and growth of ZnMoO₄ crystals. / Galashov, E. N.; Galkin, P. S.; Plusnin, P. E. и др.

В: Crystallography Reports, Том 59, № 2, 03.2014, стр. 288-290.

Результат исследования: Научные публикации в периодических изданиях › статья › рецензирование

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T1 - Specific features of the phase formation, synthesis, and growth of ZnMoO4 crystals

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AU - Shlegel, V. N.

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AB - The ZnO-MoO3 phase diagram in the range of ZnO compositions from 0.95 to 1.05 mol % is refined by differential scanning calorimetry. Data on crystal stoichiometry are obtained using the weighting method by reducing ZnMoO4 in a hydrogen atmosphere. The specific features of solid-phase synthesis of ZnMoO4 are studied, and its heat of fusion is measured. The modes of solid-phase synthesis and growth of ZnMoO4 crystals are optimized. Some experimental data on the ZnMoO4 crystal growth in the [001] direction by the low-thermal gradient Czochralski method are presented. Crystals with a cross section of ∼50 × 50 mm2, a length of 160 mm, and a weight up to 1 kg have been obtained.

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