Pseudomacrobicyclic phthalocyaninate-capped cobalt(iii) tris-pyridineoximates: Template synthesis, x-ray structure and spectral characteristics

Svetlana A. Belova, Semyon V. Dudkin, Alexander S. Belov, Yulia V. Nelyubina, Valentin V. Novikov, Yan V. Zubavichus, Yan Z. Voloshin

Результат исследования: Научные публикации в периодических изданияхстатьярецензирование

Аннотация

First pseudomacrobicyclic phthalocyaninate-capped cobalt(III) tris-pyridineoximates were obtained in moderate yields (40-49%) by the direct template condensation of 2-acetylpyridineoxime with zirconium(IV) and hafnium(IV) phthalocyaninates on the cobalt ion as a matrix. These complexes were thoroughly characterized using elemental analysis, MALDI-TOF mass-spectrometry, NMR and UV-Vis spectroscopies and by the single-crystal X-ray diffraction. Their electrochemical behaviour was studied byusing the cyclic and differential pulse voltammetries.

Язык оригиналаанглийский
Страницы (с-по)193-197
Число страниц5
ЖурналMacroheterocycles
Том12
Номер выпуска2
DOI
СостояниеОпубликовано - 2019
Опубликовано для внешнего пользованияДа

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