One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol

Kseniya S. Kovaleva; Olga I. Yarovaya; Dmitriy S. Fadeev; Nariman F. Salakhutdinov

doi:10.1016/j.tetlet.2017.03.090

One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol

Kseniya S. Kovaleva, Olga I. Yarovaya, Dmitriy S. Fadeev, Nariman F. Salakhutdinov

Результат исследования: Научные публикации в периодических изданиях › статья

1 Цитирования (Scopus)

Аннотация

The three-component condensation reaction of primary amines, formaldehyde and 2-mercaptoethanol using salts of transition and rare earth metals as catalysts was developed to obtain a new 7-membered heterocyclic structural building block, 1,5,3-oxathiazepanes, in good to excellent yields. The structure of the heterocyclic fragment was confirmed by NMR spectroscopy.

Язык оригинала	английский
Страницы (с-по)	1868-1870
Число страниц	3
Журнал	Tetrahedron Letters
Том	58
Номер выпуска	19
DOI	https://doi.org/10.1016/j.tetlet.2017.03.090
Состояние	Опубликовано - 10 мая 2017

Доступ к документу

10.1016/j.tetlet.2017.03.090

Link to publication in Scopus

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Цитировать

Kovaleva, K. S., Yarovaya, O. I., Fadeev, D. S., & Salakhutdinov, N. F. (2017). One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol. Tetrahedron Letters, 58(19), 1868-1870. https://doi.org/10.1016/j.tetlet.2017.03.090

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abstract = "The three-component condensation reaction of primary amines, formaldehyde and 2-mercaptoethanol using salts of transition and rare earth metals as catalysts was developed to obtain a new 7-membered heterocyclic structural building block, 1,5,3-oxathiazepanes, in good to excellent yields. The structure of the heterocyclic fragment was confirmed by NMR spectroscopy.",

keywords = "1,5,3-Oxathiazepanes, 7-Membered heterocycles, One-pot synthesis, Three-component reaction, MULTICOMPONENT REACTIONS, ANTI-HIV ACTIVITY, EFFICIENT SYNTHESIS, DERIVATIVES, CATALYSTS",

author = "Kovaleva, {Kseniya S.} and Yarovaya, {Olga I.} and Fadeev, {Dmitriy S.} and Salakhutdinov, {Nariman F.}",

year = "2017",

month = may,

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One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol. / Kovaleva, Kseniya S.; Yarovaya, Olga I.; Fadeev, Dmitriy S.; Salakhutdinov, Nariman F.

В: Tetrahedron Letters, Том 58, № 19, 10.05.2017, стр. 1868-1870.

Результат исследования: Научные публикации в периодических изданиях › статья

TY - JOUR

T1 - One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol

AU - Kovaleva, Kseniya S.

AU - Yarovaya, Olga I.

AU - Fadeev, Dmitriy S.

AU - Salakhutdinov, Nariman F.

PY - 2017/5/10

Y1 - 2017/5/10

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AB - The three-component condensation reaction of primary amines, formaldehyde and 2-mercaptoethanol using salts of transition and rare earth metals as catalysts was developed to obtain a new 7-membered heterocyclic structural building block, 1,5,3-oxathiazepanes, in good to excellent yields. The structure of the heterocyclic fragment was confirmed by NMR spectroscopy.

KW - 1,5,3-Oxathiazepanes

KW - 7-Membered heterocycles

KW - One-pot synthesis

KW - Three-component reaction

KW - MULTICOMPONENT REACTIONS

KW - ANTI-HIV ACTIVITY

KW - EFFICIENT SYNTHESIS

KW - DERIVATIVES

KW - CATALYSTS

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M3 - Article

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SP - 1868

EP - 1870

JO - Tetrahedron Letters

JF - Tetrahedron Letters

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