Crystal structures of [M(Еn)3](ReO4)2 (M = Ni, Zn)

S. P. Khranenko; E. A. Bykova; A. V. Zadesenets; S. A. Gromilov

doi:10.1134/S0022476617010139

Crystal structures of [M(Еn)₃](ReO₄)₂ (M = Ni, Zn)

S. P. Khranenko, E. A. Bykova, A. V. Zadesenets, S. A. Gromilov

Результат исследования: Научные публикации в периодических изданиях › статья

2 Цитирования (Scopus)

Аннотация

The structures of two isostructural phases of [M(Еn)₃](ReO₄)₂ (M = Ni, Zn; Еn is ethylenediamine) are studied. The crystal structures belong to the triclinic system, but demonstrate a pseudohexagonal packing motif. It is shown that the product of thermal decomposition of [Zn(Еn)₃](ReO₄)₂ (hydrogen atmosphere, 400 °C) is a homogeneous mixture of nanocrystalline zinc and rhenium powders with coherent scattering regions of ~30 nm.

Язык оригинала	английский
Страницы (с-по)	90-96
Число страниц	7
Журнал	Journal of Structural Chemistry
Том	58
Номер выпуска	1
DOI	https://doi.org/10.1134/S0022476617010139
Состояние	Опубликовано - 1 янв 2017

Доступ к документу

10.1134/S0022476617010139

Link to publication in Scopus

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Цитировать

Khranenko, S. P., Bykova, E. A., Zadesenets, A. V., & Gromilov, S. A. (2017). Crystal structures of [M(Еn)₃](ReO₄)₂ (M = Ni, Zn). Journal of Structural Chemistry, 58(1), 90-96. https://doi.org/10.1134/S0022476617010139

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AU - Khranenko, S. P.

AU - Bykova, E. A.

AU - Zadesenets, A. V.

AU - Gromilov, S. A.

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AB - The structures of two isostructural phases of [M(Еn)3](ReO4)2 (M = Ni, Zn; Еn is ethylenediamine) are studied. The crystal structures belong to the triclinic system, but demonstrate a pseudohexagonal packing motif. It is shown that the product of thermal decomposition of [Zn(Еn)3](ReO4)2 (hydrogen atmosphere, 400 °C) is a homogeneous mixture of nanocrystalline zinc and rhenium powders with coherent scattering regions of ~30 nm.

KW - crystal chemistry

KW - ethylenediamine

KW - nickel

KW - rhenium

KW - single crystal X-ray diffraction study

KW - zinc

KW - THERMOLYSIS

KW - THERMAL-PROPERTIES

KW - SOLID-SOLUTIONS

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DO - 10.1134/S0022476617010139

M3 - Article

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JF - Journal of Structural Chemistry

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