Crystal structure of tris-(dipivaloylmethanato) (ethylendiamine)yttrium(III)

S. A. Mosyagina; N. V. Kuratieva; K. V. Zherikova

doi:10.1134/S0022476617080108

Crystal structure of tris-(dipivaloylmethanato) (ethylendiamine)yttrium(III)

S. A. Mosyagina, N. V. Kuratieva, K. V. Zherikova

Результат исследования: Научные публикации в периодических изданиях › статья › рецензирование

Аннотация

The structure of a mixed-ligand complex tris-(dipivaloylmethanato)(ethylendiamine)yttrium(III) [Y(en)(dpm)₃] is studied at 150(2) K by single crystal XRD. The crystallographic data for C₃₅H₆₅N₂O₆Y are as follows: space group P2₁/c, a = 10.3771(3) Å, b = 26.3566(8) Å, c = 14.8412(4) Å, β = 100.385(2)°, V = 3992.6(2) Å³, Z = 4. The structure is molecular. The coordination environment of yttrium atoms is square antiprismatic; the Y–О distances are 2.2597(13)-2.3760(12) Å and Y–N distances are 2.5381(16) Å and 2.5499(17) Å.

Язык оригинала	английский
Страницы (с-по)	1546-1550
Число страниц	5
Журнал	Journal of Structural Chemistry
Том	58
Номер выпуска	8
DOI	https://doi.org/10.1134/S0022476617080108
Состояние	Опубликовано - 1 дек. 2017

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10.1134/S0022476617080108

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@article{71c63dded22b422c906d8299f2819da4,

title = "Crystal structure of tris-(dipivaloylmethanato) (ethylendiamine)yttrium(III)",

abstract = "The structure of a mixed-ligand complex tris-(dipivaloylmethanato)(ethylendiamine)yttrium(III) [Y(en)(dpm)3] is studied at 150(2) K by single crystal XRD. The crystallographic data for C35H65N2O6Y are as follows: space group P21/c, a = 10.3771(3) {\AA}, b = 26.3566(8) {\AA}, c = 14.8412(4) {\AA}, β = 100.385(2)°, V = 3992.6(2) {\AA}3, Z = 4. The structure is molecular. The coordination environment of yttrium atoms is square antiprismatic; the Y–О distances are 2.2597(13)-2.3760(12) {\AA} and Y–N distances are 2.5381(16) {\AA} and 2.5499(17) {\AA}.",

keywords = "dipivaloylmethane, ethylendiamine, single crystal X-ray diffraction analysis, synthesis, yttrium, THIN-FILMS, DEPOSITION, ZR, HEXAFLUOROACETYLACETONATE, LIGAND, PRECURSORS, MOCVD",

author = "Mosyagina, {S. A.} and Kuratieva, {N. V.} and Zherikova, {K. V.}",

year = "2017",

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Crystal structure of tris-(dipivaloylmethanato) (ethylendiamine)yttrium(III). / Mosyagina, S. A.; Kuratieva, N. V.; Zherikova, K. V.

В: Journal of Structural Chemistry, Том 58, № 8, 01.12.2017, стр. 1546-1550.

Результат исследования: Научные публикации в периодических изданиях › статья › рецензирование

TY - JOUR

T1 - Crystal structure of tris-(dipivaloylmethanato) (ethylendiamine)yttrium(III)

AU - Mosyagina, S. A.

AU - Kuratieva, N. V.

AU - Zherikova, K. V.

PY - 2017/12/1

Y1 - 2017/12/1

N2 - The structure of a mixed-ligand complex tris-(dipivaloylmethanato)(ethylendiamine)yttrium(III) [Y(en)(dpm)3] is studied at 150(2) K by single crystal XRD. The crystallographic data for C35H65N2O6Y are as follows: space group P21/c, a = 10.3771(3) Å, b = 26.3566(8) Å, c = 14.8412(4) Å, β = 100.385(2)°, V = 3992.6(2) Å3, Z = 4. The structure is molecular. The coordination environment of yttrium atoms is square antiprismatic; the Y–О distances are 2.2597(13)-2.3760(12) Å and Y–N distances are 2.5381(16) Å and 2.5499(17) Å.

AB - The structure of a mixed-ligand complex tris-(dipivaloylmethanato)(ethylendiamine)yttrium(III) [Y(en)(dpm)3] is studied at 150(2) K by single crystal XRD. The crystallographic data for C35H65N2O6Y are as follows: space group P21/c, a = 10.3771(3) Å, b = 26.3566(8) Å, c = 14.8412(4) Å, β = 100.385(2)°, V = 3992.6(2) Å3, Z = 4. The structure is molecular. The coordination environment of yttrium atoms is square antiprismatic; the Y–О distances are 2.2597(13)-2.3760(12) Å and Y–N distances are 2.5381(16) Å and 2.5499(17) Å.

KW - dipivaloylmethane

KW - ethylendiamine

KW - single crystal X-ray diffraction analysis

KW - synthesis

KW - yttrium

KW - THIN-FILMS

KW - DEPOSITION

KW - ZR

KW - HEXAFLUOROACETYLACETONATE

KW - LIGAND

KW - PRECURSORS

KW - MOCVD

UR - http://www.scopus.com/inward/record.url?scp=85041625519&partnerID=8YFLogxK

U2 - 10.1134/S0022476617080108

DO - 10.1134/S0022476617080108

M3 - Article

AN - SCOPUS:85041625519

VL - 58

SP - 1546

EP - 1550

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 8

ER -

Crystal structure of tris-(dipivaloylmethanato) (ethylendiamine)yttrium(III)

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