Selective laser melting of Zn-Si-substituted hydroxyapatite

N. Bulina; A. Titkov; D. D. Isaev; S. Makarova; S. G. Baev; A. M. Vorobyev; V. P. Bessmeltsev; N. Z. Lyakhov

doi:10.1007/s11172-021-3270-8

Selective laser melting of Zn-Si-substituted hydroxyapatite

Переведенное название: Селективное лазерное плавление Zn-Si-замещенного гидроксиапатита

N. Bulina, A. Titkov, D. D. Isaev, S. Makarova, S. G. Baev, A. M. Vorobyev, V. P. Bessmeltsev, N. Z. Lyakhov

Результат исследования: Научные публикации в периодических изданиях › статья › рецензирование

Аннотация

Впервые исследовано поведение гидроксиапатита, содержащего ионы цинка и ортосиликата, при его селективном плавлении под воздействием лазерного излучения с длиной волны 10.6 мкм. Проведен сравнительный анализ поведения данного материала при нагревании в высокотемпературной печи. Установлено, что, в отличие от режима медленного нагревания в печи, нагрев синтезированного материала со степенью замещения х = 0.2 путем сканирования пятном лазерного луча позволяет осуществить его перекристаллизацию с сохранением ионов-заместителей в структуре апатита. При больших степенях замещения (х = 1, 2) гидроксиапатиты нестабильны при обоих способах нагрева; разные условия нагрева приводят к формированию разных примесных фаз.

Переведенное название	Селективное лазерное плавление Zn-Si-замещенного гидроксиапатита
Язык оригинала	английский
Номер статьи	7
Страницы (с-по)	1682-1689
Число страниц	8
Журнал	Russian Chemical Bulletin
Том	70
Номер выпуска	9
DOI	https://doi.org/10.1007/s11172-021-3270-8
Состояние	Опубликовано - сен 2021
Опубликовано для внешнего пользования	Да

Предметные области OECD FOS+WOS

1.04 ХИМИЧЕСКИЕ НАУКИ

ГРНТИ

02 ФИЛОСОФИЯ

Доступ к документу

10.1007/s11172-021-3270-8

Другие файлы и ссылки

Fingerprint

Подробные сведения о темах исследования «Селективное лазерное плавление Zn-Si-замещенного гидроксиапатита». Вместе они формируют уникальный семантический отпечаток (fingerprint).

Цитировать

@article{50de0bbbc1174b9fa70560d33a506b29,

title = "Selective laser melting of Zn-Si-substituted hydroxyapatite",

abstract = "The behavior of hydroxyapatite containing zinc and silicate ions during selective laser melting under irradiation at 10.6 µm was studied for the first time. For comparison, the behavior of the material heated in a high-temperature furnace was investigated. It was found that, in contrast to the slow heating in the furnace, heating of the mechanochemically synthesized material with the degree of substitution x = 0.2 by scanning the laser spot enables its recrystallization with retention of substituent ions in the apatite structure. At high degrees of substitution (x = 1, 2), hydroxyapatites are unstable under both heating regimes. Different heating conditions lead to the formation of different impurity phases.",

keywords = "selective laser melting, hydroxyapatite, zinc, silicon, substitution, 3D, PHOSPHATE, CERAMICS",

author = "N. Bulina and A. Titkov and Isaev, {D. D.} and S. Makarova and Baev, {S. G.} and Vorobyev, {A. M.} and Bessmeltsev, {V. P.} and Lyakhov, {N. Z.}",

note = "Funding Information: This work was carried out within the framework of the State Assignment to the Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of the Russian Academy of Sciences (Project No. AAAA-A17-117030310277-6) and with the financial support from the Russian Foundation for Basic Research (Project No. 18-29-11064). Publisher Copyright: {\textcopyright} 2021, Springer Science+Business Media LLC.",

year = "2021",

month = sep,

doi = "10.1007/s11172-021-3270-8",

language = "English",

volume = "70",

pages = "1682--1689",

journal = "Russian Chemical Bulletin",

issn = "1066-5285",

publisher = "Springer Nature",

number = "9",

}

Selective laser melting of Zn-Si-substituted hydroxyapatite. / Bulina, N.; Titkov, A.; Isaev, D. D.; Makarova, S.; Baev, S. G.; Vorobyev, A. M.; Bessmeltsev, V. P.; Lyakhov, N. Z.

В: Russian Chemical Bulletin, Том 70, № 9, 7, 09.2021, стр. 1682-1689.

Результат исследования: Научные публикации в периодических изданиях › статья › рецензирование

TY - JOUR

T1 - Selective laser melting of Zn-Si-substituted hydroxyapatite

AU - Bulina, N.

AU - Titkov, A.

AU - Isaev, D. D.

AU - Makarova, S.

AU - Baev, S. G.

AU - Vorobyev, A. M.

AU - Bessmeltsev, V. P.

AU - Lyakhov, N. Z.

N1 - Funding Information: This work was carried out within the framework of the State Assignment to the Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of the Russian Academy of Sciences (Project No. AAAA-A17-117030310277-6) and with the financial support from the Russian Foundation for Basic Research (Project No. 18-29-11064). Publisher Copyright: © 2021, Springer Science+Business Media LLC.

PY - 2021/9

Y1 - 2021/9

N2 - The behavior of hydroxyapatite containing zinc and silicate ions during selective laser melting under irradiation at 10.6 µm was studied for the first time. For comparison, the behavior of the material heated in a high-temperature furnace was investigated. It was found that, in contrast to the slow heating in the furnace, heating of the mechanochemically synthesized material with the degree of substitution x = 0.2 by scanning the laser spot enables its recrystallization with retention of substituent ions in the apatite structure. At high degrees of substitution (x = 1, 2), hydroxyapatites are unstable under both heating regimes. Different heating conditions lead to the formation of different impurity phases.

AB - The behavior of hydroxyapatite containing zinc and silicate ions during selective laser melting under irradiation at 10.6 µm was studied for the first time. For comparison, the behavior of the material heated in a high-temperature furnace was investigated. It was found that, in contrast to the slow heating in the furnace, heating of the mechanochemically synthesized material with the degree of substitution x = 0.2 by scanning the laser spot enables its recrystallization with retention of substituent ions in the apatite structure. At high degrees of substitution (x = 1, 2), hydroxyapatites are unstable under both heating regimes. Different heating conditions lead to the formation of different impurity phases.

KW - selective laser melting

KW - hydroxyapatite

KW - zinc

KW - silicon

KW - substitution

KW - 3D

KW - PHOSPHATE

KW - CERAMICS

UR - http://www.scopus.com/inward/record.url?scp=85118210400&partnerID=8YFLogxK

UR - https://elibrary.ru/item.asp?id=47518815

U2 - 10.1007/s11172-021-3270-8

DO - 10.1007/s11172-021-3270-8

M3 - Article

VL - 70

SP - 1682

EP - 1689

JO - Russian Chemical Bulletin

JF - Russian Chemical Bulletin

SN - 1066-5285

IS - 9

M1 - 7

ER -