Synthesis of Stoichiometric and Substituted ss-Tricalciumphosphate Using Mechanochemistry

M. Chaikina, N. Bulina, O. B. Vinokurova, I. Yu Prosanov

Research output: Contribution to journalArticlepeer-review

Abstract

A solid-phase method was developed for the synthesis of ss-tricalciumphosphate (ss-TCP) with the stoichiometric composition and with partial substitution of calcium ions for copper, zinc and silver ions. The method involves preliminary preparation of precursors by means of mechanical activation of reaction mixtures. The start of ss-TCP formation was detected directly during the activation of reaction mixtures in the mill. The optimal conditions for activation, the temperature and the duration of annealing were determined.

Original languageEnglish
Pages (from-to)71-76
Number of pages6
JournalChemistry for Sustainable Development
Volume28
Issue number1
DOIs
Publication statusPublished - 2020

Keywords

  • ss-tricalciumphosphate
  • synthesis
  • mechanical activation
  • precursor
  • PHOSPHATE

OECD FOS+WOS

  • 2.04 CHEMICAL ENGINEERING
  • 1.05 EARTH AND RELATED ENVIRONMENTAL SCIENCES

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