Synthesis and Features of Crystal Structure of Scandium Hexa(isothiocyanato)chromate(III) Complex with Nicotinic Acid

E. V. Cherkasova, N. V. Pervukhina, N. V. Kuratieva, T. G. Cherkasova

Research output: Contribution to journalArticlepeer-review

Abstract

A double complex compound with a polymeric cation of composition [Sc2(C6H5NO2)3(C6H4NO2)3][Cr(NCS)6] has been synthesized by the reaction between Sc(NO3)3, K3[Cr(NCS)6], and nicotinic acid (C5H5NCOO) in an aqueous solution and studied by chemical analysis, IR spectroscopy, and X-ray diffraction. Crystals are hexagonal, space group P6322, Z = 2; a = 12.995(2) Å, c = 17.864(3) Å, V = 2612.3(7) Å3, ρcalc = 1.559 g/cm3.

Original languageEnglish
Pages (from-to)776-780
Number of pages5
JournalRussian Journal of Inorganic Chemistry
Volume63
Issue number6
DOIs
Publication statusPublished - 1 Jun 2018

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