К вопросу о точности определения параметров элементарной ячейки монокристаллов на современных лабораторных дифрактометрах

Translated title of the contribution: On the accuracy of determining unit cell parameters of single crystals on modern laboratory diffractometers

Research output: Contribution to journalArticlepeer-review

Abstract

We propose a technique for the refinement of unit cell parameters (UCPs) using a single crystal diffractometer equipped with a flat-panel area detector. The technique is based on choosing Kα1 components of X-ray radiation when processing diffraction reflections. The capabilities of the technique are demonstrated on [NiEn3]MoO4 single crystals. In two independent experiments, the difference between 2θexp and 2θcalc did not exceed 0.02° while the reproducibility of unit cell parameters was at least 0.008 Å.
Translated title of the contributionOn the accuracy of determining unit cell parameters of single crystals on modern laboratory diffractometers
Original languageRussian
Article number4
Pages (from-to)734-744
Number of pages11
Journal Журнал структурной химии
Volume62
Issue number5
DOIs
Publication statusPublished - May 2021

OECD FOS+WOS

  • 1.04 CHEMICAL SCIENCES

State classification of scientific and technological information

  • 31 CHEMISTRY

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